TA Instruments

AR1768-0001f

28/03/2013 09:27:06

Sample name	DI 40 mm AL P80B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1768
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 09:27:06

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	4.512	-79.644	10000	20.0	5.906	31.000	-6.338	9.024	-0.7023	9400	2.2529	115.4	4.5059	450.59	3.411E-3	0.0	0.5
2.0000	10.09	13.371	10000	20.0	5.906	32.000	1.064	20.17	0.05275	9400	13.5596	23.10	27.119	2711.9	3.411E-3	0.0	0.5
3.0000	15.56	25.260	10000	20.0	5.905	33.000	2.010	31.12	0.06459	9398	27.1611	9.704	54.322	5432.2	3.411E-3	0.1	0.6
4.0040	18.49	33.076	10000	20.0	5.904	34.004	2.632	36.97	0.07119	9396	41.1791	6.874	82.358	8235.8	3.411E-3	0.1	0.6
5.0000	24.70	51.927	10000	20.0	5.901	35.000	4.132	49.41	0.08363	9393	67.8629	3.847	135.73	13573	3.411E-3	0.1	0.6
6.0000	31.61	77.263	10000	20.0	5.894	36.000	6.148	63.22	0.09726	9380	106.8650	2.347	213.73	21373	3.411E-3	0.1	0.6
7.0000	34.05	87.297	10000	20.0	5.890	37.000	6.947	68.10	0.1020	9375	127.9880	2.021	255.98	25598	3.411E-3	0.1	0.6
8.0000	39.31	110.39	10000	20.0	5.890	38.000	8.784	78.62	0.1117	9373	165.4790	1.517	330.96	33096	3.411E-3	0.1	0.6
9.0080	46.03	143.60	10000	20.0	5.881	39.008	11.43	92.06	0.1241	9360	223.1220	1.104	446.24	44624	3.411E-3	0.2	0.7
10.000	50.95	171.88	10000	20.0	5.871	40.000	13.68	101.9	0.1342	9344	275.0350	0.8998	550.07	55007	3.411E-3	0.2	0.7
11.000	55.71	202.05	10000	20.0	5.870	41.000	16.08	111.4	0.1443	9342	326.0210	0.7524	652.04	65204	3.411E-3	0.2	0.7
12.000	60.09	229.42	10000	20.0	5.862	42.000	18.26	120.2	0.1519	9330	377.1220	0.6460	754.24	75424	3.411E-3	0.2	0.7
13.000	64.40	262.90	10000	20.0	5.856	43.000	20.92	128.8	0.1624	9320	434.6770	0.5617	869.35	86935	3.411E-3	0.2	0.7
14.008	69.14	297.45	10000	20.0	5.850	44.008	23.67	138.3	0.1712	9311	498.5510	0.4869	997.10	99710	3.411E-3	0.2	0.7
15.000	75.67	351.73	10000	20.0	5.839	45.000	27.99	151.3	0.1849	9292	594.0440	0.4057	1188.1	1.1881E5	3.411E-3	0.3	0.8
16.000	79.92	388.38	10000	20.0	5.831	46.000	30.91	159.8	0.1934	9281	664.0920	0.3633	1328.2	1.3282E5	3.411E-3	0.3	0.8
17.000	84.52	430.85	10000	20.0	5.817	47.000	34.29	169.0	0.2028	9258	740.4870	0.3240	1481.0	1.4810E5	3.411E-3	0.3	0.8
18.000	90.97	492.56	10000	20.0	5.804	48.000	39.20	181.9	0.2154	9238	855.2990	0.2790	1710.6	1.7106E5	3.411E-3	0.3	0.8
19.004	95.02	534.94	10000	20.0	5.794	49.004	42.57	190.0	0.2240	9221	931.0370	0.2553	1862.1	1.8621E5	3.411E-3	0.3	0.8
20.000	99.39	583.27	10000	20.0	5.777	50.000	46.42	198.8	0.2335	9195	1020.0000	0.2327	2040.0	2.0400E5	3.411E-3	0.3	0.8
20.996	105.8	651.83	10000	20.0	5.764	50.996	51.87	211.6	0.2451	9174	1153.6899	0.2048	2307.4	2.3074E5	3.411E-3	0.3	0.8
22.000	109.9	703.39	10000	20.0	5.747	52.000	55.97	219.8	0.2547	9147	1242.1000	0.1894	2484.2	2.4842E5	3.411E-3	0.4	0.9
23.004	114.2	753.49	10000	20.0	5.727	53.004	59.96	228.5	0.2624	9114	1343.4000	0.1746	2686.8	2.6868E5	3.411E-3	0.4	0.9
24.012	120.6	831.99	10000	20.0	5.710	54.012	66.21	241.3	0.2744	9088	1495.4900	0.1561	2991.0	2.9910E5	3.411E-3	0.4	0.9
25.000	124.7	894.22	10000	20.0	5.692	55.000	71.16	249.4	0.2853	9059	1596.7900	0.1456	3193.6	3.1936E5	3.411E-3	0.4	0.9
26.000	129.0	940.24	10000	20.0	5.681	56.000	74.82	258.1	0.2899	9042	1711.3500	0.1357	3422.7	3.4227E5	3.411E-3	0.4	0.9
27.004	135.4	1042.1	10000	20.0	5.650	57.004	82.93	270.9	0.3061	8992	1883.0500	0.1226	3766.1	3.7661E5	3.411E-3	0.5	1.0
28.000	139.5	1096.0	10000	20.0	5.633	58.000	87.22	279.1	0.3125	8966	1995.5500	0.1151	3991.1	3.9911E5	3.411E-3	0.5	1.0
29.004	143.6	1157.7	10000	20.0	5.619	59.004	92.12	287.3	0.3207	8942	2116.7300	0.1084	4233.5	4.2335E5	3.411E-3	0.5	1.0
30.000	150.0	1262.0	10000	20.0	5.588	60.000	100.4	300.1	0.3347	8894	2305.5000	0.09878	4611.0	4.6110E5	3.411E-3	0.5	1.0
31.000	154.1	1328.7	10000	20.0	5.571	61.000	105.7	308.3	0.3430	8866	2431.9299	0.09328	4863.9	4.8639E5	3.411E-3	0.5	1.0
32.000	158.3	1393.1	10000	20.0	5.559	62.000	110.9	316.5	0.3503	8847	2635.3799	0.08832	5270.8	5.2708E5	3.411E-3	0.5	1.0
33.000	164.6	1500.9	10000	20.0	5.515	63.000	119.4	329.3	0.3627	8777	2773.4700	0.08095	5546.9	5.5469E5	3.411E-3	0.6	1.1
34.004	168.8	1576.7	10000	20.0	5.484	64.004	125.5	337.6	0.3717	8728	2912.3301	0.07660	5824.7	5.8247E5	3.411E-3	0.6	1.1
35.000	174.9	1689.5	10000	20.0	5.452	65.000	134.4	349.7	0.3844	8677	3127.2000	0.07095	6254.4	6.2544E5	3.411E-3	0.6	1.1
36.000	179.1	1764.3	10000	20.0	5.438	66.000	140.4	358.2	0.3919	8655	3278.9500	0.06745	6557.9	6.5579E5	3.411E-3	0.6	1.1
36.996	183.3	1846.5	10000	20.0	5.416	66.996	146.9	366.5	0.4009	8619	3430.4900	0.06416	6861.0	6.8610E5	3.411E-3	0.6	1.1
38.000	189.3	1967.2	10000	20.0	5.389	68.000	156.5	378.6	0.4134	8577	3657.8301	0.05983	7315.7	7.3157E5	3.411E-3	0.6	1.1
39.004	193.4	2037.4	10000	20.0	5.345	69.004	162.1	386.9	0.4191	8506	3822.0100	0.05683	7644.0	7.6440E5	3.411E-3	0.7	1.2
40.000	199.6	2168.7	10000	20.0	5.326	70.000	172.6	399.3	0.4322	8477	4068.3401	0.05317	8136.7	8.1367E5	3.411E-3	0.7	1.2
41.000	203.7	2259.0	10000	20.0	5.292	71.000	179.8	407.4	0.4413	8423	4232.2798	0.05076	8464.6	8.4646E5	3.411E-3	0.7	1.2
42.000	207.9	2325.9	10000	20.0	5.266	72.000	185.1	415.7	0.4452	8381	4409.2900	0.04850	8818.6	8.8186E5	3.411E-3	0.7	1.2
43.000	214.0	2473.9	10000	20.0	5.230	73.000	196.9	428.1	0.4599	8324	4674.5698	0.04542	9349.1	9.3491E5	3.411E-3	0.7	1.2
44.004	218.2	2570.6	10000	20.0	5.209	74.004	204.6	436.3	0.4688	8290	4851.7598	0.04355	9703.5	9.7035E5	3.411E-3	0.7	1.2
45.000	224.3	2694.1	10000	20.0	5.126	75.000	214.4	448.6	0.4779	8158	5128.3701	0.04055	10257	1.0257E6	3.411E-3	0.8	1.3
46.000	228.4	2794.4	10000	20.0	5.111	76.000	222.4	456.8	0.4868	8134	5324.6099	0.03898	10649	1.0649E6	3.411E-3	0.8	1.3
47.000	234.5	2914.3	10000	20.0	5.076	77.000	231.9	468.9	0.4946	8078	5601.4502	0.03674	11203	1.1203E6	3.411E-3	0.8	1.3
48.000	238.5	3011.1	10000	20.0	5.037	78.000	239.6	477.0	0.5024	8016	5797.0698	0.03523	11594	1.1594E6	3.411E-3	0.8	1.3
49.008	242.6	3120.7	10000	20.0	5.009	79.008	248.3	485.3	0.5117	7972	5999.1001	0.03385	11998	1.1998E6	3.411E-3	0.8	1.3
50.000	248.8	3253.3	10000	20.0	4.940	80.000	258.9	497.5	0.5204	7862	6301.7798	0.03176	12604	1.2604E6	3.411E-3	0.8	1.3
51.000	252.8	3359.1	10000	20.0	4.902	81.000	267.3	505.6	0.5287	7802	6509.7998	0.03053	13020	1.3020E6	3.411E-3	0.9	1.4
52.000	259.1	3491.0	10000	20.0	4.895	82.000	277.8	518.1	0.5362	7791	6831.5898	0.02902	13663	1.3663E6	3.411E-3	0.9	1.4
53.004	263.1	3612.8	10000	20.0	4.829	83.004	287.5	526.1	0.5464	7686	7046.0898	0.02777	14092	1.4092E6	3.411E-3	0.9	1.4
54.004	269.1	3786.7	10000	20.0	4.771	84.004	301.3	538.2	0.5599	7593	7373.9199	0.02621	14748	1.4748E6	3.411E-3	0.9	1.4
55.000	273.3	3903.9	10000	20.0	4.759	85.000	310.7	546.5	0.5684	7574	7601.0000	0.02536	15202	1.5202E6	3.411E-3	0.9	1.4
56.000	277.4	3966.5	10000	20.0	4.692	86.000	315.6	554.7	0.5690	7468	7827.8599	0.02427	15656	1.5656E6	3.411E-3	0.9	1.4
57.000	283.3	4180.9	10000	20.0	4.669	87.000	332.7	566.7	0.5871	7431	8168.1802	0.02314	16336	1.6336E6	3.411E-3	1.0	1.5
58.000	287.5	4290.1	10000	20.0	4.622	88.000	341.4	575.0	0.5938	7357	8407.7998	0.02225	16816	1.6816E6	3.411E-3	1.0	1.5
59.004	293.6	4466.1	10000	20.0	4.567	89.004	355.4	587.2	0.6053	7269	8767.2598	0.02108	17535	1.7535E6	3.411E-3	1.0	1.5
60.000	297.6	4618.6	10000	20.0	4.556	90.000	367.5	595.1	0.6176	7250	9006.7002	0.02047	18013	1.8013E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	300.0	4627.7	10000	20.0	4.462	92.008	368.3	600.0	0.6137	7102	266.8650	0.01973	533.73	53373	3.411E-3	0.0	1.5
2.0080	300.0	4673.4	10000	20.0	4.511	93.008	371.9	600.0	0.6198	7179	518.2240	0.01994	1036.4	1.0364E5	3.411E-3	0.0	1.6
3.0080	300.0	4675.8	10000	20.0	4.507	94.008	372.1	600.0	0.6202	7173	895.5410	0.01993	1791.1	1.7911E5	3.411E-3	0.1	1.6
4.0120	300.0	4652.2	10000	20.0	4.495	95.012	370.2	600.0	0.6170	7154	1146.7000	0.01987	2293.4	2.2934E5	3.411E-3	0.1	1.6
4.9920	300.0	4656.3	10000	20.0	4.532	95.992	370.5	600.0	0.6175	7213	1524.7500	0.02003	3049.5	3.0495E5	3.411E-3	0.1	1.6
6.0080	300.0	4627.7	10000	20.0	4.451	97.008	368.3	600.0	0.6138	7084	1775.1200	0.01968	3550.2	3.5502E5	3.411E-3	0.1	1.6
6.9920	300.0	4652.4	10000	20.0	4.498	97.992	370.2	600.0	0.6170	7159	2026.3101	0.01988	4052.6	4.0526E5	3.411E-3	0.1	1.6
7.9920	300.0	4654.3	10000	20.0	4.534	98.992	370.4	600.0	0.6173	7216	2407.6599	0.02005	4815.3	4.8153E5	3.411E-3	0.1	1.6
8.9920	300.0	4643.6	10000	20.0	4.541	99.992	369.5	600.0	0.6159	7227	2654.4800	0.02008	5309.0	5.3090E5	3.411E-3	0.1	1.7
10.016	300.0	4652.5	10000	20.0	4.517	101.016	370.2	600.0	0.6170	7188	3031.5500	0.01997	6063.1	6.0631E5	3.411E-3	0.2	1.7
11.008	300.0	4644.6	10000	20.0	4.485	102.008	369.6	600.0	0.6160	7138	3285.2400	0.01983	6570.5	6.5705E5	3.411E-3	0.2	1.7
11.992	300.0	4622.6	10000	20.0	4.492	102.992	367.9	600.0	0.6131	7149	3536.2200	0.01986	7072.4	7.0724E5	3.411E-3	0.2	1.7
12.996	300.0	4626.9	10000	20.0	4.509	103.996	368.2	600.0	0.6136	7176	3921.6201	0.01993	7843.2	7.8432E5	3.411E-3	0.2	1.7
13.996	300.0	4669.5	10000	20.0	4.571	104.996	371.6	600.0	0.6193	7275	4162.4399	0.02021	8324.9	8.3249E5	3.411E-3	0.2	1.7
15.008	300.0	4629.3	10000	20.0	4.560	106.008	368.4	600.0	0.6140	7257	4542.3799	0.02016	9084.8	9.0848E5	3.411E-3	0.3	1.8
16.008	300.0	4661.5	10000	20.0	4.494	107.008	370.9	600.0	0.6183	7152	4790.8901	0.01987	9581.8	9.5818E5	3.411E-3	0.3	1.8
16.992	300.0	4640.1	10000	20.0	4.480	107.992	369.2	600.0	0.6154	7131	5044.5098	0.01981	10089	1.0089E6	3.411E-3	0.3	1.8
18.008	300.0	4673.8	10000	20.0	4.543	109.008	371.9	600.0	0.6199	7231	5420.6201	0.02009	10841	1.0841E6	3.411E-3	0.3	1.8
19.012	300.0	4650.5	10000	20.0	4.488	110.012	370.1	600.0	0.6168	7142	5670.5098	0.01984	11341	1.1341E6	3.411E-3	0.3	1.8
19.992	300.0	4647.2	10000	20.0	4.518	110.992	369.8	600.0	0.6163	7190	5921.8999	0.01997	11844	1.1844E6	3.411E-3	0.3	1.8
21.008	300.0	4635.8	10000	20.0	4.487	112.008	368.9	600.0	0.6148	7141	6301.8999	0.01983	12604	1.2604E6	3.411E-3	0.4	1.9
21.992	300.0	4628.4	10000	20.0	4.449	112.992	368.3	600.0	0.6139	7081	6550.0400	0.01967	13100	1.3100E6	3.411E-3	0.4	1.9
23.012	300.0	4638.5	10000	20.0	4.471	114.012	369.1	600.0	0.6152	7116	6927.1299	0.01977	13854	1.3854E6	3.411E-3	0.4	1.9
23.992	300.0	4664.0	10000	20.0	4.508	114.992	371.1	600.0	0.6186	7175	7181.9502	0.01993	14364	1.4364E6	3.411E-3	0.4	1.9
24.992	300.0	4635.7	10000	20.0	4.525	115.992	368.9	600.0	0.6149	7203	7429.8999	0.02001	14860	1.4860E6	3.411E-3	0.4	1.9
26.008	300.0	4633.9	10000	20.0	4.451	117.008	368.8	600.0	0.6146	7084	7808.3701	0.01968	15617	1.5617E6	3.411E-3	0.4	2.0
27.008	300.0	4632.7	10000	20.0	4.502	118.008	368.7	600.0	0.6144	7164	8058.2402	0.01990	16116	1.6116E6	3.411E-3	0.5	2.0
28.008	300.0	4610.3	10000	20.0	4.462	119.008	366.9	600.0	0.6115	7101	8436.5596	0.01973	16873	1.6873E6	3.411E-3	0.5	2.0
29.016	300.0	4647.3	10000	20.0	4.489	120.016	369.8	600.0	0.6163	7145	8686.3301	0.01984	17373	1.7373E6	3.411E-3	0.5	2.0
30.008	300.0	4637.8	10000	20.0	4.467	121.008	369.1	600.0	0.6151	7110	8937.8701	0.01975	17876	1.7876E6	3.411E-3	0.5	2.0
30.992	300.0	4659.0	10000	20.0	4.517	121.992	370.7	600.1	0.6178	7189	9316.5703	0.01997	18633	1.8633E6	3.411E-3	0.5	2.0
32.008	300.0	4638.2	10000	20.0	4.500	123.008	369.1	600.0	0.6151	7162	9566.0596	0.01989	19132	1.9132E6	3.411E-3	0.5	2.1
33.008	300.0	4645.5	10000	20.0	4.507	124.008	369.7	600.0	0.6161	7173	9945.9004	0.01992	19892	1.9892E6	3.411E-3	0.6	2.1
33.992	300.0	4638.6	10000	20.0	4.488	124.992	369.1	600.0	0.6152	7143	10198.000	0.01984	20396	2.0396E6	3.411E-3	0.6	2.1
35.008	300.0	4669.1	10000	20.0	4.533	126.008	371.6	600.0	0.6193	7214	10449.400	0.02004	20899	2.0899E6	3.411E-3	0.6	2.1
35.992	300.0	4644.2	10000	20.0	4.481	126.992	369.6	600.0	0.6160	7131	10826.400	0.01981	21653	2.1653E6	3.411E-3	0.6	2.1
36.992	300.0	4625.0	10000	20.0	4.488	127.992	368.0	600.0	0.6134	7142	11074.100	0.01984	22148	2.2148E6	3.411E-3	0.6	2.1
38.008	300.0	4646.9	10000	20.0	4.502	129.008	369.8	600.0	0.6163	7165	11325.500	0.01991	22651	2.2651E6	3.411E-3	0.6	2.2
39.012	300.0	4658.1	10000	20.0	4.488	130.012	370.7	600.0	0.6178	7143	11706.200	0.01984	23412	2.3412E6	3.411E-3	0.7	2.2
40.008	300.0	4636.4	10000	20.0	4.488	131.008	368.9	600.0	0.6149	7142	11957.600	0.01984	23915	2.3915E6	3.411E-3	0.7	2.2
40.996	300.0	4645.9	10000	20.0	4.503	131.996	369.7	600.0	0.6162	7167	12332.000	0.01991	24664	2.4664E6	3.411E-3	0.7	2.2
42.008	300.0	4628.2	10000	20.0	4.513	133.008	368.3	600.0	0.6138	7183	12582.000	0.01995	25164	2.5164E6	3.411E-3	0.7	2.2
42.992	300.0	4637.0	10000	20.0	4.493	133.992	369.0	600.0	0.6150	7151	12837.000	0.01987	25674	2.5674E6	3.411E-3	0.7	2.2
44.012	300.0	4612.0	10000	20.0	4.484	135.012	367.0	600.1	0.6116	7137	13211.400	0.01982	26423	2.6423E6	3.411E-3	0.7	2.3
44.992	300.0	4633.3	10000	20.0	4.486	135.992	368.7	600.0	0.6145	7140	13461.700	0.01983	26923	2.6923E6	3.411E-3	0.7	2.3
45.992	300.0	4671.3	10000	20.0	4.525	136.992	371.7	600.0	0.6195	7203	13712.900	0.02001	27426	2.7426E6	3.411E-3	0.8	2.3
46.992	300.0	4653.9	10000	20.0	4.512	137.992	370.3	600.0	0.6172	7182	14089.900	0.01995	28180	2.8180E6	3.411E-3	0.8	2.3
47.992	300.0	4641.8	10000	20.0	4.467	138.992	369.4	600.0	0.6156	7109	14342.900	0.01975	28686	2.8686E6	3.411E-3	0.8	2.3
48.992	300.0	4655.9	10000	20.0	4.515	139.992	370.5	600.0	0.6175	7185	14718.300	0.01996	29437	2.9437E6	3.411E-3	0.8	2.3
49.992	300.0	4610.2	10000	20.0	4.466	140.992	366.9	600.0	0.6114	7107	14969.600	0.01974	29939	2.9939E6	3.411E-3	0.8	2.3
51.008	300.0	4643.6	10000	20.0	4.509	142.008	369.5	600.0	0.6159	7177	15221.000	0.01994	30442	3.0442E6	3.411E-3	0.9	2.4
52.008	300.0	4647.1	10000	20.0	4.537	143.008	369.8	600.0	0.6163	7221	15600.000	0.02006	31200	3.1200E6	3.411E-3	0.9	2.4
52.992	300.0	4646.9	10000	20.0	4.515	143.992	369.8	600.0	0.6163	7185	15849.300	0.01996	31699	3.1699E6	3.411E-3	0.9	2.4
53.996	300.0	4645.0	10000	20.0	4.472	144.996	369.6	600.0	0.6160	7117	16227.400	0.01977	32455	3.2455E6	3.411E-3	0.9	2.4
55.004	300.0	4654.5	10000	20.0	4.528	146.004	370.4	600.0	0.6173	7206	16478.900	0.02002	32958	3.2958E6	3.411E-3	0.9	2.4
55.992	300.0	4641.3	10000	20.0	4.486	146.992	369.3	600.0	0.6156	7140	16732.301	0.01983	33465	3.3465E6	3.411E-3	0.9	2.4
56.988	300.0	4659.5	10000	20.0	4.485	147.988	370.8	600.0	0.6180	7138	17107.400	0.01983	34215	3.4215E6	3.411E-3	0.9	2.5
57.992	300.0	4668.9	10000	20.0	4.537	148.992	371.5	599.9	0.6193	7221	17357.199	0.02006	34714	3.4714E6	3.411E-3	1.0	2.5
59.016	300.0	4656.6	10000	20.0	4.512	150.016	370.6	600.0	0.6176	7181	17734.100	0.01994	35468	3.5468E6	3.411E-3	1.0	2.5
60.004	300.0	4674.5	10000	20.0	4.501	151.004	372.0	600.0	0.6200	7163	17985.500	0.01990	35971	3.5971E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	297.6	4544.2	10000	20.0	4.515	152.004	361.6	595.1	0.6076	7186	232.3960	0.02029	464.79	46479	3.411E-3	0.0	2.5
2.0040	291.5	4370.3	10000	20.0	4.558	153.004	347.8	583.0	0.5966	7254	588.0240	0.02134	1176.0	1.1760E5	3.411E-3	0.0	2.6
3.0040	287.5	4258.9	10000	20.0	4.619	154.004	338.9	574.9	0.5895	7352	825.9140	0.02224	1651.8	1.6518E5	3.411E-3	0.1	2.6
4.0200	281.3	4096.4	10000	20.0	4.659	155.020	326.0	562.6	0.5794	7415	1176.8800	0.02343	2353.8	2.3538E5	3.411E-3	0.1	2.6
5.0200	277.3	4038.0	10000	20.0	4.752	156.020	321.3	554.5	0.5795	7562	1402.1500	0.02459	2804.3	2.8043E5	3.411E-3	0.1	2.6
6.0040	273.2	3876.8	10000	20.0	4.739	157.004	308.5	546.5	0.5645	7542	1627.5200	0.02525	3255.0	3.2550E5	3.411E-3	0.1	2.6
7.0040	267.0	3744.7	10000	20.0	4.810	158.004	298.0	534.1	0.5579	7655	1965.5900	0.02684	3931.2	3.9312E5	3.411E-3	0.1	2.6
8.0040	263.0	3615.8	10000	20.0	4.829	159.004	287.7	526.0	0.5470	7686	2178.7100	0.02778	4357.4	4.3574E5	3.411E-3	0.1	2.7
9.0040	256.9	3471.0	10000	20.0	4.872	160.004	276.2	513.8	0.5376	7754	2497.8201	0.02937	4995.6	4.9956E5	3.411E-3	0.2	2.7
10.008	252.8	3373.1	10000	20.0	4.948	161.008	268.4	505.6	0.5309	7874	2710.6299	0.03080	5421.3	5.4213E5	3.411E-3	0.2	2.7
11.016	246.7	3187.6	10000	20.0	4.950	162.016	253.7	493.3	0.5142	7879	3017.2400	0.03237	6034.5	6.0345E5	3.411E-3	0.2	2.7
12.004	242.6	3094.3	10000	20.0	4.973	163.004	246.2	485.2	0.5075	7914	3217.5500	0.03362	6435.1	6.4351E5	3.411E-3	0.2	2.7
13.004	238.5	2980.0	10000	20.0	5.023	164.004	237.1	477.0	0.4972	7995	3417.8899	0.03514	6835.8	6.8358E5	3.411E-3	0.2	2.7
14.004	232.4	2874.7	10000	20.0	5.088	165.004	228.8	464.7	0.4923	8098	3705.6599	0.03750	7411.3	7.4113E5	3.411E-3	0.2	2.8
15.004	228.3	2767.7	10000	20.0	5.102	166.004	220.2	456.6	0.4824	8120	3893.3501	0.03894	7786.7	7.7867E5	3.411E-3	0.3	2.8
16.000	222.1	2628.7	10000	20.0	5.150	167.000	209.2	444.2	0.4709	8197	4174.9600	0.04154	8349.9	8.3499E5	3.411E-3	0.3	2.8
17.004	218.0	2528.4	10000	20.0	5.181	168.004	201.2	436.0	0.4615	8246	4356.2998	0.04339	8712.6	8.7126E5	3.411E-3	0.3	2.8
18.004	211.9	2408.1	10000	20.0	5.237	169.004	191.6	423.8	0.4521	8335	4621.6401	0.04640	9243.3	9.2433E5	3.411E-3	0.3	2.8
19.008	207.8	2338.3	10000	20.0	5.243	170.008	186.1	415.6	0.4478	8345	4794.6499	0.04832	9589.3	9.5893E5	3.411E-3	0.3	2.8
20.024	203.6	2255.2	10000	20.0	5.271	171.024	179.5	407.1	0.4408	8389	4969.2100	0.05062	9938.4	9.9384E5	3.411E-3	0.3	2.9
21.024	197.5	2108.5	10000	20.0	5.302	172.024	167.8	394.9	0.4249	8439	5213.2300	0.05411	10426	1.0426E6	3.411E-3	0.4	2.9
22.020	193.4	2033.3	10000	20.0	5.335	173.020	161.8	386.7	0.4184	8491	5376.4702	0.05678	10753	1.0753E6	3.411E-3	0.4	2.9
23.004	189.1	1940.5	10000	20.0	5.367	174.004	154.4	378.3	0.4082	8542	5538.1099	0.05969	11076	1.1076E6	3.411E-3	0.4	2.9
24.004	183.1	1851.7	10000	20.0	5.410	175.004	147.4	366.1	0.4025	8610	5763.3398	0.06424	11527	1.1527E6	3.411E-3	0.4	2.9
25.004	179.0	1745.8	10000	20.0	5.422	176.004	138.9	358.0	0.3881	8629	5913.2100	0.06733	11826	1.1826E6	3.411E-3	0.4	2.9
26.020	172.6	1631.4	10000	20.0	5.434	177.020	129.8	345.2	0.3760	8649	6138.2998	0.07256	12277	1.2277E6	3.411E-3	0.4	3.0
27.004	168.6	1553.9	10000	20.0	5.484	178.004	123.7	337.1	0.3668	8728	6275.6899	0.07679	12551	1.2551E6	3.411E-3	0.5	3.0
28.004	162.4	1479.8	10000	20.0	5.512	179.004	117.8	324.8	0.3626	8773	6483.5498	0.08316	12967	1.2967E6	3.411E-3	0.5	3.0
29.000	158.1	1379.1	10000	20.0	5.540	180.000	109.7	316.3	0.3470	8817	6619.2002	0.08813	13238	1.3238E6	3.411E-3	0.5	3.0
30.004	154.1	1310.8	10000	20.0	5.544	181.004	104.3	308.2	0.3385	8824	6744.1299	0.09292	13488	1.3488E6	3.411E-3	0.5	3.0
31.004	147.9	1228.0	10000	20.0	5.583	182.004	97.72	295.9	0.3303	8885	6932.1802	0.1015	13864	1.3864E6	3.411E-3	0.5	3.0
32.020	143.7	1153.5	10000	20.0	5.612	183.020	91.79	287.4	0.3194	8931	7056.2100	0.1081	14112	1.4112E6	3.411E-3	0.5	3.1
33.004	139.5	1084.1	10000	20.0	5.622	184.004	86.27	278.9	0.3093	8948	7175.8301	0.1150	14352	1.4352E6	3.411E-3	0.6	3.1
34.004	133.3	999.32	10000	20.0	5.640	185.004	79.52	266.7	0.2982	8977	7343.2900	0.1262	14687	1.4687E6	3.411E-3	0.6	3.1
35.004	129.1	930.84	10000	20.0	5.663	186.004	74.07	258.2	0.2869	9013	7455.5000	0.1352	14911	1.4911E6	3.411E-3	0.6	3.1
36.004	124.7	870.95	10000	20.0	5.688	187.004	69.31	249.5	0.2778	9053	7568.1699	0.1455	15136	1.5136E6	3.411E-3	0.6	3.1
37.024	118.5	787.75	10000	20.0	5.703	188.024	62.69	237.0	0.2645	9077	7717.7700	0.1616	15436	1.5436E6	3.411E-3	0.6	3.1
38.020	114.3	738.93	10000	20.0	5.723	189.020	58.80	228.5	0.2573	9108	7816.9302	0.1744	15634	1.5634E6	3.411E-3	0.6	3.2
39.020	109.9	685.60	10000	20.0	5.737	190.020	54.56	219.7	0.2483	9131	7960.5400	0.1891	15921	1.5921E6	3.411E-3	0.7	3.2
40.004	103.6	609.82	10000	20.0	5.755	191.004	48.53	207.3	0.2341	9159	8048.1201	0.2132	16096	1.6096E6	3.411E-3	0.7	3.2
41.008	99.40	566.83	10000	20.0	5.771	192.008	45.11	198.8	0.2269	9184	8135.5098	0.2324	16271	1.6271E6	3.411E-3	0.7	3.2
42.004	94.97	517.55	10000	20.0	5.788	193.004	41.19	189.9	0.2168	9212	8221.4297	0.2553	16443	1.6443E6	3.411E-3	0.7	3.2
43.020	88.77	448.83	10000	20.0	5.797	194.020	35.72	177.5	0.2012	9226	8335.5996	0.2927	16671	1.6671E6	3.411E-3	0.7	3.2
44.020	84.51	417.39	10000	20.0	5.813	195.020	33.21	169.0	0.1965	9251	8407.9404	0.3239	16816	1.6816E6	3.411E-3	0.7	3.3
45.020	80.02	369.96	10000	20.0	5.820	196.020	29.44	160.0	0.1839	9262	8482.3496	0.3616	16965	1.6965E6	3.411E-3	0.8	3.3
46.020	73.42	317.58	10000	20.0	5.830	197.020	25.27	146.8	0.1721	9279	8581.4697	0.4303	17163	1.7163E6	3.411E-3	0.8	3.3
47.020	69.12	281.77	10000	20.0	5.838	198.020	22.42	138.2	0.1622	9291	8643.3896	0.4862	17287	1.7287E6	3.411E-3	0.8	3.3
48.004	64.53	254.79	10000	20.0	5.849	199.004	20.28	129.1	0.1571	9309	8705.2002	0.5589	17410	1.7410E6	3.411E-3	0.8	3.3
49.004	59.87	220.05	10000	20.0	5.856	200.004	17.51	119.7	0.1462	9320	8760.7500	0.6500	17522	1.7522E6	3.411E-3	0.8	3.3
50.004	55.63	191.30	10000	20.0	5.862	201.004	15.22	111.3	0.1368	9329	8810.1504	0.7535	17620	1.7620E6	3.411E-3	0.8	3.4
51.004	51.06	167.09	10000	20.0	5.865	202.004	13.30	102.1	0.1302	9334	8859.4902	0.8950	17719	1.7719E6	3.411E-3	0.9	3.4
52.020	43.68	127.09	10000	20.0	5.871	203.020	10.11	87.37	0.1158	9344	8926.8203	1.224	17854	1.7854E6	3.411E-3	0.9	3.4
53.004	39.29	103.13	10000	20.0	5.875	204.004	8.207	78.59	0.1044	9351	8963.5195	1.514	17927	1.7927E6	3.411E-3	0.9	3.4
54.020	34.38	81.794	10000	20.0	5.884	205.020	6.509	68.75	0.09467	9364	9000.2500	1.981	18001	1.8001E6	3.411E-3	0.9	3.4
55.016	29.19	61.201	10000	20.0	5.889	206.016	4.870	58.39	0.08341	9372	9030.2500	2.749	18061	1.8061E6	3.411E-3	0.9	3.4
56.004	24.74	45.298	10000	20.0	5.886	207.004	3.605	49.48	0.07285	9368	9054.3398	3.826	18109	1.8109E6	3.411E-3	0.9	3.5
57.004	19.39	30.242	10000	20.0	5.890	208.004	2.407	38.78	0.06206	9374	9078.1904	6.233	18156	1.8156E6	3.411E-3	1.0	3.5
58.004	16.14	22.721	10000	20.0	5.892	209.004	1.808	32.28	0.05602	9378	9089.3398	9.002	18179	1.8179E6	3.411E-3	1.0	3.5
59.004	10.92	11.268	10000	20.0	5.892	210.004	0.8967	21.84	0.04105	9377	9100.8203	19.66	18202	1.8202E6	3.411E-3	1.0	3.5
60.004	5.158	2.0649	10000	20.0	5.894	211.004	0.1643	10.32	0.01593	9381	9108.5996	88.14	18217	1.8217E6	3.411E-3	1.0	3.5

